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當前位置:首頁 > 公司動態 > 小型旋轉蒸發儀在結構上有什么特征
小型旋轉蒸發儀在結構上有什么特征
點擊次數:2032 發布時間:2018-11-10
  小型旋轉蒸發儀是實驗室廣泛應用的一種蒸發儀器。適用于回流操作、大量溶劑的快速蒸發、微量組分的濃縮和需要攪拌的反應過程等。該儀器可以密封減壓至400~600毫米汞柱;用加熱浴加熱蒸餾瓶中的溶劑,加熱溫度可接近該溶劑的沸點;同時還可進行旋轉,使溶劑形成薄膜,增大蒸發面積。此外,在冷卻器作用下,可將熱蒸氣迅速液化,加快蒸發速率。
 
  小型旋轉蒸發儀采用上*的EL氣密系統,能保持高真空度,氣液分離,無回流,采用主副雙冷凝器,確保高回收率,旋轉瓶用螺母連接,便于裝卸,收集瓶下口有放液閥,回收溶煤十分快捷,可連續進料,真空系統裝真空表,對低沸點物料可調節*工作真空度。旋轉蒸發器電子恒溫控制,水浴鍋可選擇手動或電動升降,結構合理,用料講究。
 
  小型旋轉蒸發儀可配置豎直冷凝玻璃組件或傾斜冷凝玻璃組件需另行訂制,玻璃組件分為鍍防爆膜型號和非鍍防爆膜型號。加熱鍋設有可調安全回路,可根據需要進行獨立操作,并可根據需要提供安全防護罩;設計符合人體工程學,操作方便、安全;可調升降終點識別功能,有效防止玻璃組件碰碎。
 
  小型旋轉蒸發儀的使用方法:
  1、打開低溫冷卻液循環泵。注意按電源鍵后再按下制冷鍵,降到所需溫度后開循環。
  2、打開水泵循環水。
  3、裝上蒸餾燒瓶并用夾子固定好。打開真空泵,待有一定真空后開始旋轉。
  4、調節蒸餾燒瓶高度、旋轉速度,設定適當水浴溫度。
  5、蒸完先停止旋轉,再通大氣,然后停水泵,后再取下蒸餾燒瓶。
  6、停低溫冷卻液循環泵,停水浴加熱,關閉水泵循環水,倒出接收瓶內溶劑,洗干凈緩沖球,接收瓶。

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